.85 0.60 1.19 -0.10 Self-confidence limitb 1.99 ?0.007 6.012 ?0.034 10.05 ?0.081 four.96 ?0.021 9.95 ?0.076 14.955 ?0.135 1.988 ?0.01 5.952 ?0.047 9.95 ?0.104 5.015 ?0.021 ten.06 ?0.086 14.985 ?0.Interday Precision RSD a Accuracy RE 0.38 -1.00 0.70 -0.40 0.92 -0.20 0.50 0.30 0.79 -0.80 1.16 -0.40 0.58 0.ten 0.76 -0.30 1.07 -0.70 0.47 0.40 0.83 -0.20 1.23 -0.Confidence limitb 1.98 ?0.008 5.976 ?0.042 9.98 ?0.092 5.015 ?0.025 9.92 ?0.078 14.94 ?0.173 2.002 ?0.012 five.982 ?0.045 9.93 ?0.106 5.02 ?0.024 9.98 ?0.083 14.88 ?0.abMean of six determinations; RSD : percentage relative common deviation; RE : percentage relative error. Self-assurance limit at 95 confidence level and five degrees of freedom ( = two.571).Table 4: Intraday and interday precision and accuracy data for ENF obtained by the proposed solutions.MethodAdded (g mL-1 )BCGBTB5.0 10 15 five.0 10Recovery 99.ten one hundred.20 99.40 99.30 99.50 100.Precision RSD a 0.42 0.78 1.16 0.53 0.90 1.Intraday Accuracy RE -0.90 0.20 -0.60 -0.70 -0.50 0.50 Confidence limitb 4.955 ?0.021 ten.02 ?0.078 14.91 ?0.173 four.965 ?0.026 9.95 ?0.09 20.ten ?0.231 Recovery 99.60 99.80 99.20 100.60 99.40 99.Precision RSD a 0.51 0.75 1.02 0.40 0.68 0.Interday Accuracy RE -0.40 0.20 -0.80 0.60 -0.60 -0.Self-assurance limitb 4.98 ?0.025 9.98 ?0.075 14.88 ?0.152 5.03 ?0.020 9.94 ?0.068 19.92 ?0.abMean of six determinations; RSD : percentage relative common deviation; RE : percentage relative error. Self-confidence limit at 95 self-confidence level and five degrees of freedom ( = two.571).Journal of Analytical Strategies in ChemistryJournal of Analytical Techniques in ChemistryTable five: Determination of GMF in its pharmaceutical dosage forms applying the common addition strategy.Reagent Taken (g mL-1 ) Pure drug added (g mL-1 )2.BCG2.BCP2.BPB2.BTB5.MO4.0 eight.0 12 2.0 6.0 10 4.0 8.0 12 4.0 8.0 12 5.0 10Factive tablets Flobiotic tablet GemiQue tablets Total located (g mL-1 ) Recovery a ?SD Total found (g mL-1 ) Recovery ?SD Total discovered (g mL-1 ) Recovery ?SD 5.96 99.30 ?0.78 5.98 99.60 ?0.67 6.02 one hundred.30 ?0.51 9.91 99.ten ?1.02 ten.02 100.20 ?0.82 9.92 99.20 ?0.70 13.97 99.80 ?1.2-Bromo-5-chlorothiazolo[4,5-b]pyridine Purity 24 13.RuPhos Pd G4 uses 96 99.PMID:23381626 70 ?1.09 13.99 99.90 ?0.94 three.996 99.90 ?0.66 3.96 99.ten ?0.42 three.97 99.30 ?0.38 8.02 one hundred.20 ?0.90 7.98 99.80 ?0.69 7.99 99.90 ?0.84 11.92 99.30 ?0.95 12.05 one hundred.40 ?1.03 11.95 99.60 ?1.17 five.97 99.50 ?0.57 five.99 99.80 ?0.36 six.01 one hundred.15 ?0.76 9.97 99.70 ?0.76 9.96 99.60 ?0.49 9.97 99.70 ?0.96 13.87 99.ten ?1.14 13.97 99.90 ?0.78 13.89 99.20 ?1.21 6.03 one hundred.50 ?0.48 6.01 one hundred.ten ?0.53 six.01 100.10 ?0.54 9.90 99.00 ?0.72 9.96 99.60 ?0.85 9.96 99.60 ?1.03 13.93 99.50 ?0.97 13.96 99.70 ?1.31 14.04 one hundred.30 ?1.15 9.97 99.70 ?0.32 9.91 99.ten ?0.70 9.99 99.90 ?0.65 14.94 99.60 ?0.56 15.06 one hundred.40 ?1.05 14.97 99.80 ?0.85 24.95 99.80 ?0.90 24.88 99.50 ?1.25 24.90 99.60 ?1.aAverage of six determinations.Table six: Determination of MXF in its pharmaceutical dosage forms applying the standard addition strategy.Reagent Taken (g mL-1 ) Pure drug added (g mL-1 )2.BCP2.BPB2.BTB5.MO2.0 six.0 10 four.0 eight.0 12 2.0 four.0 8.0 5.0 10Avelox tablets Moxiflox tablets Moxifloxacin tablets Total discovered (g mL-1 ) Recovery a ?SD Total identified (g mL-1 ) Recovery ?SD Total found (g mL-1 ) Recovery ?SD 3.98 99.40 ?0.56 three.96 99.ten ?0.62 three.98 99.60 ?0.48 7.98 99.70 ?0.83 8.06 100.70 ?0.89 7.98 99.80 ?1.10 11.89 99.ten ?1.20 12.02 one hundred.20 ?1.26 11.92 99.30 ?1.17 5.98 99.60 ?0.61 five.97 99.50 ?0.35 5.96 99.30 ?0.36 9.99 99.90 ?0.84 9.96 99.60 ?0.60 9.99 99.90 ?0.63 14.07 100.50 ?1.14 13.99 99.90 ?0.85 14.08 100.60 ?1.3.